Direct evidence by 31P-n.m.r. spectroscopy is presented for the formation of a five-co-ordinate intermediate in the Arbuzov reaction of tervalent phosphorus esters with elemental chlorine or elemental bromine and benzenesulphenyl chloride.
A. Skowrońska, J. Mikołajczak and J. Michalski, J. Chem. Soc., Chem. Commun., 1975, 791 DOI: 10.1039/C39750000791
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