Metal nanoparticle-decorated carbon spheres (mn-CSs) are prepared by combining one-pot hydrothermal synthesis and post-synthesis modification. The former sol–gel type process is employed to obtain heteroatom-containing polymer spheres (PSs), which easily attract metal species that, during thermal treatment, are initially converted to nanoparticle-decorated PSs and finally to mn-CSs.
N. P. Wickramaratne and M. Jaroniec, Chem. Commun., 2014, 50, 12341 DOI: 10.1039/C4CC05271D
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