Via implantation of nitrogen from aq. NH3 into hydroxymethylfurfural (HMF), dimethyl furan-2,5-dicarboximidate was synthesized over a manganese oxide catalyst. It was realized by the ammoxidation of HMF followed by methanol addition under mild reaction conditions. The imidate prepared in situ was further transformed into 2,5-furandiamidine dihydrochloride by reaction with ammonium chloride.
X. Jia, J. Ma, M. Wang, H. Ma, C. Chen and J. Xu, Green Chem., 2016, 18, 974 DOI: 10.1039/C5GC01985K
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