Issue 31, 2019
From the journal:

New Journal of Chemistry

Silver-mediated radical phosphorylation/cyclization of N-allylbenzamides to access phosphoryl-substituted dihydroisoquinolones†

Xiao-Ceng Liu,‡a   Kai Sun, ORCID logo ‡a   Qi-Yan Lv,ab   Xiao-Lan Chen, ORCID logo *a   Yuan-Qiang Sun,*a   Yu-Yu Peng,c   Ling-Bo Qua  and  Bing Yu ORCID logo *ab  

* Corresponding authors

a College of Chemistry, Zhengzhou University, Zhengzhou 450001, China
E-mail: chenxl@zzu.edu.cn, bingyu@zzu.edu.cn

b Henan Nonferrous Metals Geological Exploration Institute, Zhengzhou 450052, Henan Province, China

c Hunan Provincial Key Laboratory of Materials Protection for Electric Power and Transportation, Changsha University of Science & Technology, Changsha 410114, China

Abstract

A silver-mediated phosphorylation/cyclization of N-allylbenzamides with phosphine oxides for the synthesis of phosphoryl-substituted dihydroisoquinolones was developed. This protocol features broad substrate scope, experimental simplicity, high efficiency, step-economy, and facile scalability.

Graphical abstract: Silver-mediated radical phosphorylation/cyclization of N-allylbenzamides to access phosphoryl-substituted dihydroisoquinolones

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Article information

DOI
https://doi.org/10.1039/C9NJ02833A
Article type
Letter
Submitted
31 May 2019
Accepted
15 Jul 2019
First published
15 Jul 2019

New J. Chem., 2019,43, 12221-12224

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Silver-mediated radical phosphorylation/cyclization of N-allylbenzamides to access phosphoryl-substituted dihydroisoquinolones

X. Liu, K. Sun, Q. Lv, X. Chen, Y. Sun, Y. Peng, L. Qu and B. Yu, New J. Chem., 2019, 43, 12221 DOI: 10.1039/C9NJ02833A

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