Pyrazolyl-containing aryliodolium salts undergo transformation to iodopyrazoles accompanied by the formation of a new Csp2–Csp2 bond in the presence of a base (DIPEA, NaOH, or K2CO3). The plausible mechanism of the base-mediated reaction is suggested. The catalytic activity of the iodine-containing species is studied in the model reaction.
Y. V. Safinskaya, M. V. Il’in and D. S. Bolotin, New J. Chem., 2024, 48, 19034 DOI: 10.1039/D4NJ02894E
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