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Desilylative C(sp2)–C(sp2) cross-coupling reactions of arylsilanes with aryldiazonium salts under Au(I)/photoredox catalysis have been reported. The addition of Cu-salts as catalysts was found to be crucial for the success of this transformation.

Graphical abstract: Visible light mediated desilylative C(sp2)–C(sp2) cross-coupling reactions of arylsilanes with aryldiazonium salts under Au(i)/Au(iii) catalysis

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