A novel and efficient transformation of primary alcohols to one-carbon shorter carboxylic acids using IBX is reported. Mechanistic studies revealed that the combination of IBX and molecular iodine produces a different active hypervalent iodine species.
S. Xu, K. Itto, M. Satoh and H. Arimoto, Chem. Commun., 2014, 50, 2758 DOI: 10.1039/C3CC49160A
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