Hydrogen was efficiently evolved from glycerol aqueous solution upon vertical photoirradiation of a Pt/TiO2 or Au/TiO2 bed under aerobic conditions. Granular photocatalysts were easily deposited, leading to high H2 selectivity (80–95%), whereas glycerol oxidation with CO2 evolution became dominant when suspended powder photocatalysts were used.
H. Sakurai, M. Kiuchi, C. Heck and T. Jin, Chem. Commun., 2016, 52, 13612 DOI: 10.1039/C6CC08319F
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